| The
technique of weighing is one of the most accurate measuring
methods for experimental investigations. For numerous applications,
however, it is not possible or useful to locate a balance
or a weighing instrument in the measurering chamber itself
(e.g. at high temperatures, high pressures, aggressive atmospheres).
In many of these cases magnetic suspension balances could
be a suitable solution.
By
means of magnetic suspension balances it is possible to accurately
measure the weight changes of a sample located in a closed
measuring cell made of metal or glass. In these cases, the
balance (a commercial analytical or micro balance) is located
outside the measuring cell at ambient atmosphere and the sample
is contactlessly weighed "through the wall" of the
measuring cell. The operating principle of such magnetic suspension
balances is illustrated in the following figure.
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Operating principle of a magnetic suspension
balance.
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The
key component of the magnetic suspension balance is the magnetic
suspension coupling which consists of an electromagnet (with
a soft iron core), a suspension magnet (a permanent magnet),
a position sensor, and a control system. The electromagnet
is attached to the underfloor weighing hook of the balance
and maintains a freely suspended state of the supension magnet.
To achieve the freely suspended state of this permanent magnet,
its position is detected by a position sensor and controlled
via a direct analog control circuit. The sample is linked
to the permanent magnet via a load coupling and decoupling
device (this "measuring position" is shown in the
figure). By means of the magnetic suspension coupling, weight
changes of the sample are contactlessly transmitted to the
balance. To avoid any influence of a zero-point drift of the
balance the sample can be decoupled from the suspension magnet
by lowering it to a zero-point position (tare position) about
5 mm below the measuring position shown in the figure. Since
only the permanent magnet is weighed in this position a simple
and fast zero-point check is possible at all times. All movements
of the suspension magnet and the sample vessel are electronically
controlled so that any vibration is avoided. The measuring
accuracy at the balance is not adversely affected by the magnetic
suspension coupling.
Specifications |
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Application fields |
Load range: |
10 g / 100 g |
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• Density measurement |
Resolution: |
0.001 mg / 0.01 mg |
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• Sorption measurement |
Balances: |
Micro or analytical balances |
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• Thermogravimetry |
Pressure range: |
Vacuum bis 100 MPa |
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• Viscosity measurement |
Temperature range: |
Up to 773 K |
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• Surface tension |
Types: |
Quartz glass, metal LP/HP |
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Although
the principle of contacless weighing was already developed
more than 50 years ago, corresponding weighing instruments
could only be produced for very restricted fields of application
until the middle of the 1980s. Only by changing the control
principle decisively [71,
73]
it has been successful to develop a new type of magnetic suspension
balances that could be used for a great variety of different
applications. This new type enables the application of gravimetric
measuring methods in wide ranges of pressure and temperature
and with nearly any sample loads for the first time. The operating
principle and the fields of application of the new magnetic
suspension balance are described in detail in [71,
73]. In our laboratories,
the magnectic suspension balances are especially applied for
measurement of the density and the viscosity of fluids (see
densimeters,
combined
visco-densimeter, and research
projects for industry). The following figure shows two
photos of a demonstration model (cutaway model) of a magnetic
suspension balance (with a quartz-glass sinker for density
measurements of fluids) that has especially been built up
for the demonstration of the operating principle of a magnetic
suspension balance.
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Cutaway
model of a magnetic suspension balance.
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Since
the new magnetic suspension balances are suitable for many
different applications and there has been a great interest
of other research and metrology laboratories, magnetic suspension
balances have also been commercially available in many different
versions and for a lot of different applications for about
ten years (Rubotherm Präzisionsmesstechnik, Germany,
www.rubotherm.de).
Magnetic suspension balances are currently used in numerous
research institutes and industrial companies all over the
world.
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