SUPERCONDUCTING FT NMR Spectrometer AVANCE NEO 400 WB
Manufacturer: Bruker BioSpin GmbH, Silberstreifen 4, 76287 Rheinstetten
This spectrometer is a replacement for the old ASX 400 NMR spectrometer as part of the "Großgeräte der Länder" program of the German Research Foundation (DFG).
The new spectrometer has been in operation since November 2020.
Magnet System Ascend 400 MHz WB, Field Strength 9.39 T
AVANCE NEO 400 MHz Console
Spectrometer Console Equipment
The spectrometer equipment (400 MHz, B0= 9.39 Tesla) for 1H / 19F and X-nuclei includes:
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Magnetsystem Ascend 400 MHz WB
8.9 cm bore (field strength at 9.39 Tesla), actively shielded for minimal magnetic stray field-
EDS (External Disturbance Suppression) efficient suppression of external magnetic field disturbances (e.g. trams, trains and elevators)
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comfortable nitrogen and helium filling intervals
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Measuring probes for nitrogen and helium level measurement with alarm function
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Magnet stand with integrated vibration damping
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EDS (External Disturbance Suppression) efficient suppression of external magnetic field disturbances (e.g. trams, trains and elevators)
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Shim-Control Unit
High-precision, ultra-stable shim power board with 20 shim power sources
• 20-bit digital resolution each and +/- 1 A shim current range
# Depending on the shim system, two units are required
# the power sources are with all Bruker orthogonal and matrix shim systems
compatible (e.g. BOSS III) -
NMR Windows 10-Workstation
Computer equipped as follows:
• Intel Xeon Quad Core E5-1620v3 / 3.5 GHz
• Working memory: 16 GB RAM (2x 8GB), DDR4-2133 ECC
• Integrated SATA / 3GB / s hard disk controller, RAID 0, 1, 5, 10
• Hard disk 2 TB, 3GB / s, NCQ, SATA, 7200 rpm
• HP DVD drive, 16-speed, DVD + - / RW DL SuperMulti
• Network adapter: 1x Intel 82579 on board 10/100/1000 Mbits / s (SPECT), 1x Intel
Ethernet I210 10/100/1000 Mbits / s
• HP Optical Scroll Mouse, USB
• HP Enhanced USB Keyboard with US or UK English layout
• TopSpin software (pre-installed, license not included)
• Operating system: Windows 10 Workstation -
B-SVT Interface Probehead (T)
Adapter with connections to a suitable probe head
• two type T thermocouples
• a heating channel
• Sensor connection to prevent the probe head from overheating in the event of a gas failure protection -
B-SVT Temperature control unit
Highly integrated temperature control unit
• digital temperature sensor with a resolution <5 mK
• Temperature stability depending on the environment and probe head (e.g. 10 mK / K at
High resolution room temperature probes)
• Compatible with different types of temperature sensors (e.g. Thermocouple T or
E, PT 100)
• Gas flow monitoring up to 3,000 l / h with flow control
• Integrated anti-freeze mode for cryoprobe heads
• up to four independent heating channels (e.g. for flow probes)
• for high temperature experiments (up to 600 ° C with high temperature probes)
without additional heater
• intelligent gas flow control for easy sample feeding with different
Spinner types (ceramic, KEL-F, etc.), without manual setting (e.g. SampleCase,
SampleJet)
• Control of intelligent SmartCoolers (BCU) and low temperature accessories (LN2
Heat exchanger, evaporator)
• Exact sample temperature determination and regulation by NMR thermometer -
Amplifier BLAH1000
Single channel amplifier
• min. 1000 W HF pulse power (max. 50 W CW)
• min. 100 W HF pulse power (max. 20 W CW)
• Software-controlled switching between 100 and 1000 W HF pulse power
• Pulse program controlled 'blanking' and ultra-fast 'rise / fall' times
• Integrated computer-controlled RF amplifier protection by monitoring the
Output and reflected power
• Ethernet interface for service and NMR system integration -
Broadband Amplifier BLABB500
Single channel broadband amplifier
• min. 500 W HF pulse power at 15-600 MHz (max. 50 W CW)
• Pulse program controlled 'blanking' and ultra-fast 'rise / fall' times
• Broadband RF channel with two identical outputs that can be used if necessary
different preamplifiers can be connected (without manual
Rewiring)
• Integrated computer-controlled RF amplifier protection by monitoring the
Output and reflected power
• Ethernet interface for service and NMR system integration -
Broadband Amplifier BLABB1000
Single channel broadband amplifier
• min. 1000 W HF pulse power at 15-600 MHz (max. 50 W CW)
• Pulse program controlled 'blanking' and ultra-fast 'rise / fall' times
• Broadband RF channel with two identical outputs that can be used if necessary
different preamplifiers can be connected (without manual
Rewiring)
• Integrated computer-controlled RF amplifier protection by monitoring the
Output and reflected power
• Ethernet interface for service and NMR system integration -
GaAs-preamplifier HPLNA 1H
Linear, low-noise GaAs broadband preamplifier for observation and
Decoupling from 57Fe to 19F
• Noise figure (NF) ~ 1.4 dB including all internal filters and the active transmission
/ Reception switch
• maximum 500 W pulse power
• Calibrated at the factory for exact tuning and matching
• Integrated 1H stop filter
• for broadband probes -
Broadband preamplifier HPPR XBB19F 2HP
Linear, low-noise GaAs broadband preamplifier for observation and
Decoupling from 57Fe to 19F
• Noise figure (NF) ~ 1.4 dB including all internal filters and the active transmission
/ Reception switch
• maximum 500 W pulse power
• Calibrated at the factory for exact tuning and matching
• Integrated 1H stop filter
• for broadband probes -
Broadband preamplifier HPLNA XBB31P 2HP
Highly linear, low-noise GaAs broadband preamplifier for observation and
Decoupling from 57Fe to 31P
• Noise figure (NF) ~ 1 dB including all internal filters and the active transmission
/ Reception switch
• maximum 4 kW pulse power
• Integrated HF power detection
• Calibrated at the factory for exact tuning and matching
• Integrated 1H stop filter
• for broadband probes (e.g. MAS) that require high RF power -
Frequency channel TRX1200
Highly integrated NMR RF transmitter / receiver unit with pulse program engine
(Sequencer, waveform memory)
• RF signal width from 5 to 1200 MHz for sending and receiving
• Time resolution 12.5 ns
• Simultaneous adjustment of RF amplitude, phase and frequency within 12.5 ns
• Ultra-fast ADC, 240 MSPS @ 16 Bit, digital down converter (DDC)
• ultra-fast DAC, 960 MSPS, digital boost converter (DUC)
• high intermediate frequency (IF) of 1852 MHz for sending and receiving
• Sequencer waveform memory 1 GB (e.g. pulse shaping, optimum control
Applications, composite pulse decoupling)
• Spectral width up to 7.5 MHz
• effective dynamic range> 17 bit (5 MHz) /> 19 bit (1 MHz) /> 23 bit (6 kHz) -
MAS pneumatic Unit
Fully automatic MAS III pneumatic unit including automatic start-up and
Braking the rotors (7 mm to 0.7 mm outer diameter)
• precise regulation of the sample rotation (max. 0.25 ‰ of the respective maximum speed)
• automatic ejection with designated probes
• Trigger output for synchronization with the rotation
• Ethernet remote control for automatic operation
• Including cable and hose set
Single-channel amplifier BLAH1000,
Broadband amplifier BLABB500 and
Broadband amplifier BLABB1000
Broadband amplifier BLABB500 and
Broadband amplifier BLABB1000
Frequency channel TRX1200 and Ethernet router
Probehead equipment
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CPMAS WB double resonance probehead 7 mm
CPMAS H / X-DVT double-resonance probe head for WB solid-state NMR
• 7 mm
• X-channel tunable from 31P to 15N
• 1H high power decoupling
• Temperature range -130 ° C to 150 ° C
• Maximum rotation frequency 7 kHz, only specified for Bruker rotors -
CPMAS WB double resonance probehead 2.5 mm
CPMAS H / X-DVT double resonance probe head with extended tuning range of the
1H channel for WB solid-state NMR
• 2.5 mm
• X-channel tunable from 31P to 15N
• High power decoupling from 1H to 19F
• Temperature range -50 ° C to 80 ° C
• Maximum rotation frequency 35 kHz, only specified for Bruker rotors -
CPMAS WB triple resonance probehead 4.0 mm
CPMAS H / X / Y-DVT triple resonance probe head with extended tuning range
of the 1H channel for WB solid-state NMR
• 4 mm
• Exchangeable inserts define the tuning range of the X-channel to a fixed one
Frequency between 31P and 2H
• The tuning range of the Y-channel is determined by the frequency of the X-channel:
highest Y frequency 11B, lowest Y frequency 15N
• High power decoupling from 1H to 19F
• Temperature range -130 ° C to 150 ° C
• Maximum rotation frequency 15 kHz, only specified for Bruker rotors
• 1H / 13C / 15N insert
+ Without an insert, the probe head can be used as a double resonance probe head (X-channel
adjustable from 31P to 15N). -
CPMAS double resonance probehead 4 mm
CPMAS H / X-WVT double resonance probe head with extended temperature range
and extended tuning range of the 1H channel for WB solid-state NMR
• 4 mm
• X-channel tunable from 31P to 15N
• High power decoupling from 1H to 19F
• Temperature range -120 ° C to 300 ° C
• Maximum rotation frequency 15 kHz, only specified for Bruker rotors -
Static broadband probehead
for solid-state broad-line NMR spectroscopy
• 3 interchangeable solenoid coils (5 mm high range, 5 mm 2H frequency and 10
mm low range up to 400 MHz or 5 mm low range for 500 MHz)
• Tuning range 109Ag to 31P
• Ceramic sample chamber
• Temperature range –150° C to + 400° C -
Low temperature equipment
for operation with LN2
• 25 l LN2 dewar
• heat exchanger
• evacuated stainless steel transfer line (flexible)
• BSVT interface
• Low temperature range down to approx. -120 ° C with 5 mm probes and B-ST
# effective temperature range depending on the probe head
CPMAS H/X/Y-DV triple resonance probehead with extended tuning range
of the 1H channel for WB solid-state NMR
of the 1H channel for WB solid-state NMR
Broadband static probe head
for solid-state broad-line NMR spectroscopy
• 3 interchangeable solenoid coils (5 mm high range, 5 mm 2H frequency and 10
mm low range up to 400 MHz or 5 mm low range for 500 MHz)
for solid-state broad-line NMR spectroscopy
• 3 interchangeable solenoid coils (5 mm high range, 5 mm 2H frequency and 10
mm low range up to 400 MHz or 5 mm low range for 500 MHz)